Lab-Scale Coagulation and
Flocculation Experiments
&
Thickener Design
Jar Test
The jar test is the most common laboratory
coagulation/flocculation tests and consists of:
placing a sample of the wastewater in a jar:
rapidly adding the coagulant and intensely
mixing the sample for a short time
(coagulation/destabilization phase);
allowing the floc to form under gentle mixing
conditions (flocculation phase)
allowing the floc to sediment in the quiescent sample
(define specific settling time and rate)
comparing the turbidity of the sample with the
initial turbidity
Jar Test Apparatus
The Objectives of Jar Test
Experiment
Optimizing dosage and pH for efficient
coagulation/flocculation
The Objectives of Jar Test
Experiment
Optimizing turbidity and pH for efficient
coagulation/flocculation
The Objectives of Jar Test
Experiment
Optimizing turbidity and dose for efficient
coagulation/flocculation
The Objectives of Jar Test
Experiment
Furthermore,
The intensity of the mixing
The effect of the other counter-ions and co-ions
The effect of the aquacomplex formation
The settling rate of the suspension
The final volume of the thickened/sedimented portion
CAN BE OPTIMIZED depending on the technical
requirements.
Determination of Thickener Area
Determination of Thickener Area
THICKENER DESIGN
1ST STEP: SEDIMENTATION EXPERIMENT
IN LAB
The rate of fall of the interface between
the pulp and clarified solution being
timed.
THICKENER DESIGN
1ST STEP: SEDIMENTATION EXPERIMENT
IN LAB
THICKENER DESIGN
2ND STEP: DRAWING THE SEDIMENTATION
CURVE
MUDLINE HEIGHT VS TIME
THICKENER DESIGN
3RD STEP: FINDING CRITICAL POINT (c) & tU
THICKENER DESIGN
4TH STEP: CALCULATE THICKENER
AREA & DIAMETER
1- 2- Find tu and Calculate
UNIT AREA for thickener from
the previous sedimentation
initial height and concentration curve.
of suspension
height and concentration
of sediment at a given time (t)
THICKENER DESIGN
4TH STEP: CALCULATE THICKENER
AREA & DIAMETER
3- Calculate required total thickener area for the given capacity
(feed rate)
W : T/H
A1 C0 : T/M3
H0 : M
Tu : H
4- As an engineer, always include safety factor in such calculations!
A2 = 1.2 X A1
THICKENER DESIGN
4TH STEP: CALCULATE THICKENER
AREA & DIAMETER
5 – Calculate the diameter of thickener from the area.
W : T/H
C0 : T/M3
A1 H0 : M
Tu : H
From the calculated area,
you can find the radius and the diameter of
the thickener.
PROBLEM
CALCULATE THE REQUIRED UNIT THICKENER AREA FOR THE
SUSPENSION WHICH CONTAINS 25% solids. (C0:0.1 T/M3)
Why is the thickener design
important ?