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  BY QIRAT NOREEN 2131 RAFSHANGULZAR 2132 MEHREEN GUL 2142 BS CHEMISTRY SESSION 2021-25 SUPERVISOR : Dr. ZAFARULLAH KHAN SHAMPOO FORMULATION AND ITS PREPARATION FROM NATURAL INGREDIENTS
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  •The term Shampoois derived from Hindi word Champo meaning to press or massage. • This reflects the traditional practice in India of massaging the scalp with herbal mixture •The earliest forms of shampoo originated in the Indian subcontinent during the Indus valley civilization, over 4,000 years ago. INTRODUCTION 1
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  Types of ShampooClassified on the Basis of Consistency; 1) Clear Liquid Shampoo 2) Cream Shampoo 3) Gel Shampoo 4) Powder Shampoo 5) Aerosol Shampoo 2
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  Classification of ShampooBased on their Function a) Clarifying Shampoo b) Anti-Dandruff Shampoo c) Herbal Shampoo d) Baby Shampoo e) Medicated Shampoo f) Tea Tree Shampoo 3
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  Herbal Shampoo Benefits GentleCleansing Enhanced Hair Growth Improved Scalp Health 4
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  • Natural shampoowith gentle cleansers from plants, smoothing Amla for scalp comfort, Fenugreek extract for healthy hair. • Review scientific literature on herbal shampoo formulation and select active and auxiliary ingredients. • Develop a stable shampoo formulation and choose quality evaluation parameter. • Evaluate the quality of shampoo. Research Objectives 5
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  Materials Used DuringResearch 1) Reetha Extract. 2) Amla Extract. 3) Tulsi Extract. 4) Fenugreek Extract. 5) Ashwagandha Extract. 6) Shikakai Extract 6
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  FTIR Machine Glass beakers Measuringcylinder Filter paper Test tubes Stirrer Mortar and pestle Apparatus 7
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  • Conducted acomprehensive review of scientific literature on shampoo composition. • Developed a research work plan involving the formulation of multiple shampoo samples. • Optimized shampoo composition by experimenting with different extract. • Repeated all tests three times to ensure accuracy. • Assessed quality by measuring PH , foam volume , FTIR analysis ,texture and stability. • Repeated all tests three times to ensure accuracy. Preparation of Research Work Plan 8
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  Procedure •50 ml ofdistilled water was mixed with 10 g of Sodium Lauryl Sulphate and heated until Sodium Lauryl Sulphate dissolved. •1 g of Gelatin was added to the mixture and stirred until dissolved. •1 g of Citric Acid was added to the mixture and stirred until dissolved. •The prepared herbal extracts were added to the mixture and stirred well. •0.1g of Sodium Benzonate was added to the mixture . •The pH of shampoo was adjusted to 6.8 using Citric Acid. •The shampoo was mixed thoroughly . 9
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  Physical Appearance • Theprepared Herbal Shampoo exhibited a dark brown to light black color, depending on the concentration of Herbal extracts. • it had a pleasant herbal aroma, contributed mainly by Tulsi and 10
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  The pH ofthe shampoo was found to be 6.86, which is within the acceptable range for scalp and hair applications. pH Determination 11
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  Foam ability A 20ml of water and 2ml shampoo was poured into a 250 ml graduated cylinder and shaken. 12
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  400 900 14001900 2400 2900 3400 3900 4400 30 40 50 60 70 80 90 100 FTIR FTIR Wave Number % T FTIR Analysis of Herbal Shampoo This FTIR analysis covers a herbal shampoo formulation composed of the following ingredients: Ashwagandha, Reetha, Amla, Shikakai, Tulsi, Alcohol, Water, Fenugreek, Gelatin solution, Sodium Benzoate solution, and Sodium Lauryl Sulphate. 13
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  •Broad peaks around3200–3600 cm ¹: Indicate O–H ⁻ stretching from water, Alcohols, and Phenols (present in Tulsi, Ashwagandha, Ethanol, etc.) •Sharp peaks at 2850–2950 cm ¹: Arise from C–H stretching ⁻ in Alkanes. •Carbonyl peaks around 1650–1750 cm ¹: Represent C=O ⁻ stretches from Esters (Amla, Reetha), Amides (Gelatin), and Carboxylic acids (Amla). • Sulphate vibration at 1200-1250cm ¹; strong peak due to ⁻ SO4 -2 symmetric stretch (Sodium Lauryl Sulphate). • 14
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  Comparison with PreviousResearch • Sharma et al. (2019) formulated a shampoo using Amla, Reetha, and Shikakai. They reported a foam volume of 5-6 cm and a pH range of 5.5–6. Their formulation showed moderate foam stability. In comparison, our shampoo demonstrated superior foaming properties and greater stability, likely due to the optimized herbal blend. • Rao et al. (2022) explored the benefits of Ashwagandha in hair care and noted improvements in hair strength and shine. These effects were also observed in our study, reinforcing Ashwagandha therapeutic potential in hair care products. 15
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  CONCLUSION • The presentstudy focused on the formulation, evaluation, and comparison of an herbal shampoo composed of natural ingredients such as Ashwagandha, Reetha, Amla, Shikakai, Tulsi, and Fenugreek along with Alcohol and water as solvents. • The herbal ingredients used in the formulation were selected based on their traditional usage and scientifically proven benefits. . 16
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  • Amla isrich in Vitamin C and antioxidants that help to strengthen hair follicles. • Shikakai works as a natural cleanser and conditioner • Tulsi has antimicrobial property that helps to maintain scalp health. • The herbal shampoo developed in this research demonstrates significant potential as an effective and safe alternative to conventional Shampoos. • Reetha acts as a natural surfactant 17
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  THANks